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Two-photon polymerization with diode lasers emitting ultrashort pulses with high repetition rate
(2020)
In this Letter, we investigate the resolution of two-photon polymerization (2PP) with an amplified mode-locked external cavity diode laser with adjustable pulse length and a high repetition rate. The experimental results are analyzed with a newly developed 2PP model. Even with low pulse peak intensity, the produced structural dimensions are comparable to those generated by traditional 2PP laser sources. Thus, we show that a compact monolithic picosecond laser diode without amplification and with a repetition rate in the GHz regime can also be applied for 2PP. These results show the high application potential of compact mode-locked diode lasers for low-cost and compact 2PP systems.
This paper describes how two-photon polymerization was used to generate biomimetic nanostructures with angle-insensitive coloration inspired by the blue butterflies of Morpho. Less angle dependence was achieved by engineering the structures with a certain degree of disorder, which delimited them from classical photonic crystals. Variations in the processing parameters enabled the color hue to be controlled. In this context, blue, green, yellow, and brown structures were demonstrated. Reflection spectra of the structures were simulated and studied experimentally in a broad range of incident angles. Additionally, a molding technique was performed as a potential scale-up strategy. The application of such biomimetic structures is discussed.
In this manuscript, a new approach in surface plasmon resonance microscopy is presented. The method provides optical real-time detection of single nanoparticles on surfaces. The potential of the method is demonstrated recording spherical dielectric particles as small as 40 nm in diameter and single HIV virus-like particles having diameters of similar to 100 nm both immobilized on functionalized surfaces. The surface plasmon resonance signal in the binding spots was found to be almost linearly proportional to the size of the particles and, therefore, surpasses the intensity of Mie scattering on spherical particle (dependence similar to r(-6)) by orders of magnitude for small objects. The physical reason leading to this strong effect is discussed.
The spatially varying intensity in a standing wave resonator leads to spatial hole burning in the gain medium of a laser. The spatial hole burning changes the gain of different longitudinal modes and can thus determine the optical spectrum of the laser. We simulate this longitudinal mode competition in standing wave resonators of thin-disk lasers. The resulting optical spectra of the laser are compared to measured optical spectra. We examine two types of resonators: I-resonators and V-resonators with different angles of incidence. In V-resonators, the non-normal incidence of the laser beam on the disk lifts the degeneracy of the polarization. Experiments show that the slight gain advantage for the p-polarization does not lead to polarized emission. For both types of resonators, the measured spectra are in good agreement with the simulated ones. The simulations allow to study the influence of spectral intra-cavity losses on the optical spectrum of a thin-disk laser.
The Anatomy of Glenoid Concavity-Bony and Osteochondral Assessment of a Stability-Related Parameter
(2021)
The need for portable and on site screening methods for viruses is evident in face of virus infections that can spread lastly in a heavily connected world. A robust and efficient method for detecting viruses is a novel technique called Plasmon Assisted Microscopy of Nanoobjects. It is based on the acquisition of images from a sensor surface exploiting the behavior of surface plasmons in the presence of nanoobjects. In this paper an efficient image analysis approach with respect to the requirements of the sensor is presented and an embedded image processing system for this purpose is introduced. The processing pipeline comprises three steps and starts with restorating the images by removing the background and filtering artifacts. The acquired image series is analyzed pixel by pixel in a second pipeline step in order to detect pixels containing nanoobjects. In a last step pixels are aggregated to nanoobject structures. The paper introduces in the context of this virus detection method a configurable embedded system that was used for rapid prototyping of the image analysis algorithms in a flexible way. (C) 2010 Elsevier B.V. All rights reserved.
The laser nitriding was performed in nitrogen gas at room temperature (20 °C) and low temperature (−190 °C) by a low power fiber laser to modify the wear and abrasion resistance of NiTi alloy. The surface roughness and element composition were analyzed by roughness device and energy-dispersive X-ray spectroscopy respectively. The results of roughness show that laser treatment can change the surface roughness due to the laser remelting. The effect of laser nitriding on the microhardness, friction coefficient, and worn scars of NiTi alloy was also studied, which shows that the microhardness of the NiTi alloy increases after laser nitriding. The optical microscope and scanning electron microscope were used to characterize the surface of NiTi alloy after wear testing to observe the microstructure of worn scars. The results show that the laser nitriding with different parameters can induce a nitride layer with different thicknesses and the higher energy deposition is the key factor for the formation of the nitride layer, which can decrease the friction coefficient and reduce wear loss during the application of NiTi alloy. The improvement of wear resistance can be attributed to the hard nitriding layer.
High strength steel has been used in the aviation industry and automotive body structural applications to reduce its mass through a reduction in thickness. Therefore, it is very important to enhance its mechanical property, such as microhardness. In the present research, the high strength steel samples were treated by laser shock peening (LSP) with different laser pulse energy and laser pulse width. The microhardness and residual stress were measured to compare the difference between laser energy of 3 J with 10 ns and 5 J with 20 ns. The results in the study show that the surface LSP treatment can increase the microhardness and the compressive residual stress can be found when the samples were tested by hole drilling testing.
This research paper presents the attempt at ultrashort pulsed laser shock peening with absence of absorptive layer and confining medium which could enhance surface microhardness and the abrasion property of NiTi shape memory alloy. The average roughness values of NiTi specimen were measured on the surface, because the roughness would affect the friction resistance. The microhardness and Young's modulus were investigated at different position of single laser spot by nanoindentation technique. The pin-on-plate sliding abrasion testing were performed with different load-force (0.5 N and 2 N) for different testing time. Results showed that ultrashort pulsed laser shock peening treatment would cause a significant improvement on friction coefficient and abrasion property, which was attributed to the change of surface modification, such as roughness, microhardness, microstructure and titanium oxide layer …
Laser shock peening with femtosecond laser was used to improve the corrosion resistance of biomedical NiTi alloy without protective coating in the air environment. The energy dispersive X-ray analysis (EDX) and X-ray diffraction (XRD) based analysis showed that the laser ablation could produce titanium oxide layer and femtosecond laser shock peening (FsLSP) can generate residual stress in the surface layer of NiTi alloy. The FsLSP improved the corrosion resistance of NiTi in 3.5% NaCl solution and Hank’s solution and also prevented the formation of corrosion cracks and pits during corrosion testing. The reasons for the improvement of corrosion behavior may be the generation of residual stress and titanium oxide film during the laser surface treatment.
The experiment study presents the influence of femtosecond laser shock peening (FsLSP) without a protective layer in the air on the surface hardness and surface mechanical property of NiTi shape memory alloy. Femtosecond laser shock peening is a new possibility of direct laser ablation without any protective layer under atmospheric conditions, which can produce intense shock waves with low pulse energy in the air. The average surface roughness values of the NiTi alloy samples were measured, because the surface roughness may affect its friction resistance. The results showed that the surface roughness of NiTi increased after femtosecond laser shock peening treatment. In comparison with the initial state, the coefficient of friction decreased and surface microhardness increased after femtosecond laser shock peening treatment with different FsLSP parameters. This improvement of wear properties may be attributed to the enhancement of surface microhardness and surface titanium oxide layer induced by the shock wave and laser ablation during FsLSP treatment.
Laser shock peening with a femtosecond laser system was presented in this research work. The NiTi shape memory alloy was processed by the femtosecond laser shock peening (FsLSP) treatment without a protective layer in the air. Femtosecond laser shock peening is a new surface technology, which can induce an intense shock wave with low single laser pulse energy under atmospheric conditions. The surface topography, roughness, microhardness, and wear resistance were measured on the surface of NiTi alloy before and after femtosecond laser peening treatment. The results showed that the surface roughness and microhardness could be increased after femtosecond laser shock peening, which may be due to the laser ablation and micro-plastic deformation induced by the shock wave. The wear property of NiTi alloy was improved, which may be attributed to the FsLSPed surface texturing and …
Laser shock peening is a new and important surface treatment technique that can enhance the mechanical properties of metal materials. Normally, the nanosecond laser with pulse-width between 5 ns and 20 ns is used to induce a high-pressure shock wave that can generate plastic deformation in the top layer of metals. The femtosecond laser shock peening in the air has been studied recently, which can induce higher pressure shock wave than that of traditional nanosecond laser shock peening in a very short time. The NiTi alloy is processed by femtosecond laser shock peening, then a nanoindentation device is used to measure its surface hardness and residual stress. The hardness results of NiTi alloy before and after treatment show that the femtosecond laser shock peening can increase the hardness of NiTi alloy, which also shows that the femtosecond laser can be used to perform laser shock peening on NiTi alloy without coating.
We present, to the best of our knowledge, the first intracavity pumped Yb:YAG thin-disk laser. It operates at 1050.7 nm with a quantum defect of just 1.74% due to pumping at 1032.4 nm. Low absorption of the pump light at the pump wavelength of 1032.4 nm is compensated for by placing the disk inside the resonator of another Yb:YAG thin-disk laser which is diode-pumped at 940 nm. The intra-cavity pumped laser has an output power of 10.3 W and a slope efficiency of 8.3%
We present a novel pump concept that should lead to single-frequency operation of thin-disk lasers without the need for etalons or other spectral filters. The single-frequency operation is due to matching the standing wave pattern of partially coherent pump light to the standing wave pattern of the laser light inside the disk. The output power and the optical efficiency of our novel pump concept are compared with conventional pumping. The feasibility of our pump concept was shown in previous experiments.
Adaption of the NDIR-technology to 13CO2-breath tests under increased inspiratory O2 concentrations
(2009)
It has been shown that the beam quality and the efficiency of high-power solid-state lasers could be enhanced by the use of deformable mirrors in order to compensate for optical aberrations. An intracavity compensation requires a deformable mirror which is capable of handling very high laser intensities. The active diameter of the deformable mirror should be a few millimeters in order to match typical fundamental mode laser beam diameters. There is a wide variety of commercially available deformable mirrors, but neither meets all requirements.
Novel unimorph deformable mirror with monolithic tip-tilt functionality for solid state lasers
(2011)
We present a new type of unimorph deformable mirror with monolithic tip-tilt functionality. The tip-tilt actuation is based on a spiral arm design. The mirror will be used in high-power laser resonators for real-time intracavity phase control. The additional tip-tilt correction with a stroke up to 6 μm simplifies the resonator alignment significantly. The mirror is optimized for a laser beam footprint of about 10 mm. We have modeled and optimized this mirror by finite element calculations and we will present design criteria and tradeoffs for this mirrors. The mirror is manufactured from a super-polished glass substrate with very low surface scattering and excellent dielectric coating.
Over the past 5 years we have developed a new type of unimorph deformable mirror. The main advantages of this mirror technology are · very low surface scattering due to the use of superpolished glass · excellent coatings, even suitable for high power lasers, can be applied · active diameter of the mirrors can be between 10 mm and 100 mm · large strokes can be achieved even for small mirror diameters · integrated monolithic tip/tilt functionality based on a spiral arm design We have modeled these mirrors by analytical models as well as by the finite element method. This allows us to quickly design new mirrors tailored to specific applications. One example is a mirror for laser applications that has a diameter of 10 mm and can achieve a stroke in defocus mode of 5 μm. The stroke for these mirrors scales as the square of the mirror diameter, meaning that we can achieve, for example, a stroke of 125 μm for a mirror of 50 mm diameter. We will present design criteria and tradeoffs for these mirrors. We characterize our mirrors by the maximum stroke they can deliver for various Zernike modes, under the boundary condition that the Zernike mode has to be created with a certain fidelity, usually defined by the Maréchal criterion.
We present a novel unimorph deformable mirror with a diameter of only 10 mm that will be used in adaptive resonators of high power solid state lasers. The relationship between applied voltage and deformation of a unimorph mirror depends on the piezoelectric material properties, layer thicknesses, boundary conditions, and the electrode pattern. An analytical equation for the deflection of the piezoelectric unimorph structure is derived, based on the electro-elastic and thin plate theory. The validity of the proposed analytical model has been proven by numerical finite-element modelling and experimental results. Our mirror design has been optimized to obtain the highest possible stroke and a high resonance frequency.
We have developed a new type of unimorph deformable mirror, designed to correct for low-order Zernike modes. The mirror has a clear optical aperture of 50 mm combined with large peak-to-valley Zernike amplitudes of up to 35 μm. Newly developed fabrication processes allow the use of prefabricated super-polished and coated glass substrates. The mirror's unique features suggest the use in several stronomical applications like the precompensation of atmospheric aberrations seen by laser beacons and the use in woofer-tweeter systems. Additionally, the design enables an efficient correction of the inevitable wavefront error imposed by the floppy structure of primary mirrors in future large space-based telescopes. We have modeled the mirror by using analytical as well as finite element models. We will present design, key features and manufacturing steps of the deformable mirror.