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Adaption of the NDIR-technology to 13CO2-breath tests under increased inspiratory O2 concentrations
(2009)
We present a novel unimorph deformable mirror with a diameter of only 10 mm that will be used in adaptive resonators of high power solid state lasers. The relationship between applied voltage and deformation of a unimorph mirror depends on the piezoelectric material properties, layer thicknesses, boundary conditions, and the electrode pattern. An analytical equation for the deflection of the piezoelectric unimorph structure is derived, based on the electro-elastic and thin plate theory. The validity of the proposed analytical model has been proven by numerical finite-element modelling and experimental results. Our mirror design has been optimized to obtain the highest possible stroke and a high resonance frequency.
The mechanisms of femtosecond laser-induced transient melting and atomic mixing in a target composed of a 30 nm Au film deposited on a bulk Cu substrate are investigated in a series of atomistic simulations. The relative strength and the electron temperature dependence of the electron-phonon coupling of the metals composing the layered target are identified as major factors affecting the initial energy redistribution and the location of the region(s) undergoing transient melting and resolidification. The higher strength of the electron-phonon coupling in Cu, as compared to Au, results in a preferential sub-surface heating and melting of the Cu substrate, while the overlaying Au film largely retains its original crystalline structure. The large difference in the atomic mobility in the transiently melted and crystalline regions of the target makes it possible to connect the final distributions of the components in the resolidified targets to the history of the laser-induced melting process, thus allowing for experimental verification of the computational predictions. (C) 2009 Elsevier B. V. All rights reserved.
A new simple design of a high-efficiency low-transport-time cell for laser ablation is presented. The main feature of the design is that the particles are transported by a laminar spiral gas flow into the outlet without any contact with the cell walls. The efficiency of the particle transport and the dependence of the ICP-MS peak shape on experimental conditions were measured. The peak duration on the 10% level was found to be as short as 30 ms and the transport efficiency reached 100% when analysing a standard brass sample. As an example of application to real samples with fine inhomogeneities, the profiles of C-13, Ca-44 and Pb-208 were measured by LA-ICP-MS across a tree core. As a result, the very quick particle transport time of the cell enabled the fine, seasonal variation in wood composition to be resolved.